This work reports a new technique that uses microfluidics technology for processing nanomaterials. Microchannels defined in poly-dimethyl siloxane (PDMS) using soft lithography distribute nanoparticles within a monomer solution. The solution is subsequently photo-polymerized to yield a polymer with dispersed nanoparticles, and microscopy techniques are used to characterize the material. Currently, silica nano-particles dispersed in a hydrogel have been investigated, but this technique should be applicable to other systems.